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Hanna

Coulometric Karl Fischer Titrator – HI934

Product code: MX-11398

Coulometric Karl Fischer Titrator – HI934 For scientists and professionals who need exact water content determination from 1 ppm to 5%, our new generation of the Coulometric Karl Fischer Titrator is engineered to meet or exceed your technical requirements while delivering a lower cost of ownership.

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Product description

Dynamic Titrant Dosing The titration speed feature allows for timely and accurate titration results by relating the amount of iodine generated to the mV response from the Karl Fischer reaction. Drift Rate Compensation The HI934 automatically adjusts the titration calculation to account for the effects of any ambient humidity entering the titration cell. This provides a more accurate result by correcting for water not present in the actual sample. Titration Results Averaging Successive results from a titration method may be averaged with recording of the standard deviation. Selectable Endpoint Criteria The HI934 employs a dual platinum pin electrode for bivoltammetric endpoint determination. Users may choose termination criteria based on mV stability times or drift rates. Multistage Cell Preparation A pre-titration stage eliminates residual water present in the solvent and the cell, providing a reliable baseline start to analysis. Standby mode then keeps the solvent dry between titrations and when the titrator is not in use. Titration System Precision Iodine Generation Hanna’s dosing algorithm allows for an extremely small amount of iodine necessary for the Karl Fischer reaction to be generated electrolytically using a pulsed current up to 400 mA delivering titrant accurately and precisely. Chemically Resistant Titration Vessel and Tubing The glass titration cell and PTFE tubing is designed to withstand the harsh solvents and reagents involved in Karl Fischer reactions. Sealed Solvent System Ground glass joints completely seal the glass titration cell minimizing exposure to ambient humidity, keeping the system dry, and reducing reagent consumption while saving time between titrations. Solvent may be exchanged in a matter of seconds with a quick fitting adjustment. Molecular Sieve Desiccant High efficiency molecular sieve desiccant helps maintain low and stable drift rates within the titration cell while preventing the ingress of ambient humidity into the sealed solvent system. Digital Built-in Stirrer Automatic, integrated magnetic stirrer adjustable from 200-2000 RPM with optical feedback for automatic speed control. Interface & Display Detailed Titration Graphs A real-time titration curve can be displayed during each titration; this feature is useful when new methods are tested or when a procedure requires optimization. Interactive Color Display A large, color LCD screen clearly shows the chosen titration method along with results, units, drift rate, and mV value. Simple and Quick Navigation Virtual key selections present on the display allow for simple and quick navigation between screens and menus without getting lost in a nest of information. Titrator Data & Reporting Customizable Titration Reports Each titration report is fully customizable so users can ensure they are storing and filing the appropriate data required for their application and procedures. Flexible GLP Management All necessary GLP (Good Laboratory Practice) information can be recorded with each sample including: sample identification, company and operator name, date, time, electrode ID codes, and calibration information. Effortless Data Transfer Data can easily be transferred to a USB flash drive or PC with the Hanna HI900PC application software. The USB port allows for the transfer of titration methods, titration reports, and software upgrades via USB flash drive. Methods of Analysis Customizable Methods The HI934 can store up to 100 user-defined or standard titration methods. Each method may be customized and optimized for performance based on application and user requirements.

Specifications

Titration Principlecoulometric Karl Fischer
Titration Range1 ppm to 5%
Titration Resolution0.1ppm to 0.0001%
Measurement Units%, ppm, ppt, mg/g, μ g/g, mg, μ g, mg/mL, μ g/mL, mg Br/100g, g Br/100g, mg Br, g Br
Sample Typeliquid or solid with external dissolution / extraction
Pre-Titration Conditioningautomatic
Background Drift Correctionautomatic or user-selectable value
Endpoint Criteriafixed mV persistence, relative drift stop or absolute drift stop
Dosing Typedynamic with optional pre-dispensing rate
Result Statisticsmean, standard deviation
Titration Vesseloperating volume between 100 – 200 mL
Solvent Handling Systemsealed system, integrated diaphragm air pump
Connection TypeBNC
Polarization Current1, 2, 5, or 10 μ A
mV Range2 mV to 1100 mV
mV Resolution0.1 mV
mV Accuracy±0.1%
Stirrer Typemagnetic, optically regulated, digital stirrer
Stirrer Speed200 to 2000 rpm
Stirrer Resolution100 rpm
Titrator Methodsup to 100 methods (standard and user-defined)
Reportsup to 100 complete titration reports and drift rate reports can be stored
GLP ConformityGood Laboratory Practice and instrument data storage and printing
Peripheral Devicesconnections for VGA display, PC-keyboard, parallel printer, USB device input, RS232
Display5.7” (320 x 240 pixel) color LCD
Keypadpolycarbonate
LanguagesEnglish, Portuguese. Spanish, and French
Power Supply100-240 VAC; “-01” models, US plug (type A); “-02” models, European plug (type C)
Environmentoperating
Dimensions315 x 205 x 375 mm (12.4 x 8.1 x 14.8 “)
Weightapproximate 4.3 kg (9.5 lbs.)